HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131725780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10005668 | HCID 10005668 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 131725780 | HCID 131725780 | 197.6% |
Reaction Steps
To a solution of 4-chloro-N-(4-hydroxy-benzyl)-N-[4-(2-pyrrolidin-1-yl-ethoxy)-phenyl]benzenesulfonamide (0.016 g, 32.9 μmol) in methanol (1 mL) was added HCl as a 1M solution in ether (0.045 ml). The reaction mixture was stirred at room temperature for 1 hr., and then concentrated in vacuo to give the title compound (0.017 g, 32.5 μmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053212B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-b8bc10e7ba894e0eb682844518d345e6 |
| Source note | uspto-grants-2006_05 |