O-Cresol → HCID 178428730, compound
Reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[OH:8].[N:9]([O-])=[O:10].[Na+]>>[CH3:1][C:2]1[C:3](=[O:8])[CH:4]=[CH:5][C:6](=[N:9][OH:10])[CH:7]=1Participants
3
Procedure
2-Methyl-1,4-benzoquinone-4-oxime was prepared by reaction of 2-methylphenol with sodium nitrite under acidic conditions by the method described by T. Ishikawa et al. in J. Org. Chem. 1996, 61, page 2778.
Sources & evidence
- ORD record
- ord-433b57efe700424191d4f4d364303d3e
- Source dataset
- uspto-grants-2006_06
- Patent number
- US07056349B2
Reaction notes
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