2-Chlorophenol → HCID 178516263, compound

HRID 1827628Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[OH:8].[N:9]([O-])=[O:10].[Na+]>>[Cl:1][C:2]1[C:3](=[O:8])[CH:4]=[CH:5][C:6](=[N:9][OH:10])[CH:7]=1

Participants

Reactant 2

HCID 72452-Chlorophenol

HCID 23668193Sodium Nitrite

Product 1

HCID 178516263HCID 178516263, compound

Procedure

2-Chloro-1,4-benzoquinone-4-oxime was prepared by reaction of 2-chlorophenol with sodium nitrite under acidic conditions by the method described by T. Ishikawa et al. in J. Org. Chem. 1996, 61, page 2778.

Sources & evidence

ORD record: ord-444e0be6db54411d9527b95c1782f5d9
Source dataset: uspto-grants-2006_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07056349B2

Reaction notes

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