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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1827732Generated: November 1, 2026

HCID 135724426, compound → HCID 135487799, compound

https://huagongshe.com/reaction/1827732

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 135724426HCID 135724426—
SolventAcetonitrileHCID 6342—
ProductHCID 135487799HCID 13548779987.7%

Reaction Conditions

Temperature95 °C

Reaction Steps

To 1.0 g of the compound of Example 5 was added 20 mL of acetonitrile, and the mixture was stirred upon heating on an oil bath at 95° C. for 35 minutes. The suspension was cooled to room temperature, and a precipitate was collected by filtration and rinsed with 6 mL of acetonitrile to obtain 0.85 g of the titled compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07056910B2
Source datasetuspto-grants-2006_06
ORD IDord-6c6b78eefd35497cb751689d0a207a77
Source noteuspto-grants-2006_06