HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → 2-Benzylideneamino-4-methylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 2-Amino-4-methylphenol | HCID 7264 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Benzylideneamino-4-methylphenol | HCID 11298789 | 63.9% |
Reaction Steps
A solution of 2-amino-p-cresol (1.23 g, 10 mmol) and benzaldehyde (1.06 g, 10 mmol) in methanol (10 ml) was heated at reflux for 2 hrs then cooled in an ice bath. The product was filtered off, washed with a little cold methanol and dried to yield 1.35 g of 2-benzylideneamino-4-methylphenol 54.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07056903B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-51e2b74668464f41b6df062b9d493318 |
| Source note | uspto-grants-2006_06 |