反应详情

A solution of 2-amino-p-cresol (1.23 g, 10 mmol) and benzaldehyde (1.06 g, 10 mmol) in methanol (10 ml) was heated at reflux for 2 hrs then cooled in an ice bath. The product was filtered off, washed with a little cold methanol and dried to yield 1.35 g of 2-benzylideneamino-4-methylphenol 54.

1. temperatureat reflux for 2 hrs
2. temperaturethen cooled in an ice bath
3. filtrationThe product was filtered off
4. washwashed with a little cold methanol
5. customdried