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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1828473Generated: November 2, 2026

Thionyl Chloride → HCID 22063674, compound

https://huagongshe.com/reaction/1828473

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 22063596HCID 22063596—
ProductHCID 22063674HCID 2206367496.4%

Reaction Steps

The 2-[2-(4-methoxybenzyl)-2H-1,2,3,4-tetrazol-5-yl]acetic acid (262.0 mg, 1.05 mmol) obtained in (B) was added dropwise with thionyl chloride (615.9 μl, 8.44 mmol) under ice cooling and stirred at room temperature for 30 minutes. Excessive regents were evaporated to obtain the title compound (0.27 g, quantitative) as pale yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07056917B2
Source datasetuspto-grants-2006_06
ORD IDord-08b46b59e2174ea58b9815c8042100ae
Source noteuspto-grants-2006_06