Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Phenethylamine | HCID 1001 | — |
| Product | Formamide, N-(2-phenylethyl)- | HCID 140995 | 89.1% |
Reaction Steps
A mixture of phenylethylamine (20.0 g, 0.165 mol) and formic acid (49.4 ml, 1.309 mol) was slowly heated to 200° C. Excess water and formic acid were distilled off in the process. The mixture was then kept at 200° C. for 1 hour, and the product was distilled under reduced pressure, giving a colourless oil (22.0 g, 0.147 mol, 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07060707B2 |
|---|
| Source dataset | uspto-grants-2006_06 |
|---|
| ORD ID | ord-021e98b9817348e791eec977f6caba93 |
|---|
| Source note | uspto-grants-2006_06 |
|---|
