Ammonium Hydroxide → HCID 69660224, compound

HRID 1828890Notes

Reaction equation

HRID 1828890 reaction equation
C[O:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH2:11][CH2:12][C:13]2[CH2:17][C:16](=[O:18])[NH:15][N:14]=2)=[CH:7][CH:6]=1)=O.[OH-].[NH4+:20]>>[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH2:11][CH2:12][C:13]2[CH2:17][C:16](=[O:18])[NH:15][N:14]=2)=[CH:7][CH:6]=1)(=[O:2])[NH2:20]

Participants

3

Reactant 2

HCID 14923Ammonium HydroxideHCID 69660228HCID 69660228, compound

Product 1

HCID 69660224HCID 69660224, compound

Procedure

A mixture of 3-(4-methoxycarbonylphenylethyl)-2-pyrazolin-5-one (7.7 mmol) in ammonium hydroxide 25% (30 ml), was stirred at room temperature for 12 hours. The solvent was concentrated in vacuo and the solid product formed was filtered and dried.

Workup

  1. concentrationThe solvent was concentrated in vacuo
  2. customthe solid product formed
  3. filtrationwas filtered
  4. customdried

Sources & evidence

ORD record
ord-84ddac2dbb4b424ea7bc5f5591ead237
Source dataset
uspto-grants-2006_06
Patent number
US07060822B1

Reaction notes

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