HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 22059719, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 4-(Chloroacetyl)-3,5-dimethyl-1H-pyrrole-2-carbaldehyde | HCID 22059855 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22059719 | HCID 22059719 | — |
Reaction Steps
Diethylamine (5 ml) was added to a solution of 4-(2-Chloroacetyl)-3,5-dimethylpyrrole-2-carboxaldehyde (1 g, 5 mmol) in THF (20 ml). The mixture was stirred at room temperature for 24 h. The solvent was removed under reduced pressure and the residue was treated with water, NaHCO3 (5%) and extracted with dichloromethane. After drying and filtering, the solvent was removed and the residue was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07060822B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-f5763b2445974eb093d9337134f23510 |
| Source note | uspto-grants-2006_06 |