Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → 4-(2-(Ethylamino)propyl)-1,2-benzenediol hydrobromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | [2-(3,4-Dimethoxy-phenyl)-1-methyl-ethyl]-ethyl amine | HCID 22061570 | — |
| 생성물 | 4-(2-(Ethylamino)propyl)-1,2-benzenediol hydrobromide | HCID 130356 | — |
반응 단계
A solution of 1.1 g (4.92 mmol) of 2A in 10 mL of 48% HBr was heated to reflux under argon atmosphere for 3.5 hours and then concentrated to dryness under reduced pressure. To this was added 50 mL of dichloromethane and concentrated to dryness under reduced pressure to give crude 2B as a dark brown powder (M+Na, 318).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07060847B2 |
| 출처 데이터셋 | uspto-grants-2006_06 |
| ORD ID | ord-77d7e3110a764e9292a3c1dbb67f5612 |
| 출처 메모 | uspto-grants-2006_06 |