HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 501150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 501151 | HCID 501151 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 501150 | HCID 501150 | — |
Reaction Steps
To a solution of 34.3 gm (0.1 mol) 2-[1-(2,5-dimethylphenyl) octylthio]pyridine N-oxide and 10.7 gm (0.26 mol) acetonitrile in 400 ml of methanol was added sufficient NaOH solution (6 N to minimize water) to adjust the pH in the operating range of 9.0 to 9.5 (true), approximately 11–12 (meter). 17 gm (0.26 mol) of 50% hydrogen peroxide was added in increments.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07064139B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-6f2822d255a64758898ae87d09091e1c |
| Source note | uspto-grants-2006_06 |