HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl mercaptan → HCID 501219, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | Pyridine, 3-chloro-, 1-oxide | HCID 123133 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 501219 | HCID 501219 | — |
Reaction Steps
As described in U.S. Pat. No. 4,394,155, Example 1, 2-(phenylmethylthio)-5-chloropyridine N-oxide is prepared from 5-chloropyridine N-oxide and benzylmercaptan. To a well stirred solution of 2.5 g (9.01 mol) of the thio compound in 25 mL chloroform is added 4 g (0.02 mol) of MCPBA in 50 mL chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07064139B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-5ea368f3c8144d839c98b473e99d9ec2 |
| Source note | uspto-grants-2006_06 |