Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | HCID 9894952 | HCID 9894952 | — |
| Product | HCID 10290195 | HCID 10290195 | 78% |
Reaction Steps
Compound 284 was dissolved in ethanol, 10 equivalents of ethylene diamine was added and the reaction mixture was heated at 60° C. for 15 hours. The solvent was evaporated and the target compound was purified by HPLC, the yield is 78%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07064218B2 |
|---|
| Source dataset | uspto-grants-2006_06 |
|---|
| ORD ID | ord-df3c546b505849d7a1bb287e3500f6c8 |
|---|
| Source note | uspto-grants-2006_06 |
|---|
