HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 68682576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 68678821 | HCID 68678821 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68682576 | HCID 68682576 | — |
Reaction Steps
N-[4-(1-methyl(3-piperidyloxy))-2-nitrophenyl]acetamide was dissolved in 1:1 MeOH : 6N NaOH (aq) solution (0.03 M). After stirring at room temperature for 2 hours, MeOH was removed in vacuo. The remaining solution was extracted with EtOAc (3×). The combined organic extracts were then dried over Na2SO4 and concentrated in vacuo to give 4-(1-methyl(3-piperidyloxy))-2-nitrophenylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07064215B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-2705e0f9ea13402a95064464c7cb0ff3 |
| Source note | uspto-grants-2006_06 |