HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isopropylpiperazine → HCID 22055743, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isopropylpiperazine | HCID 78013 | — |
| Reactant | 4,5-Difluoro-2-nitroaniline | HCID 157151 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22055743 | HCID 22055743 | — |
Reaction Steps
4,5-Difluoro-2-nitrophenylamine (1.0 equivalent) and N-isopropyl piperazine were heated at 100° C. for 3 hours. The solution was then cooled to room temperature and diluted with water. The resulting precipitate was filtered and dried under vacuum to provide title compound product. LC/MS (m/z) 283.2 (MH+), Rt 1.56 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07064215B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-71846b919c2849edbe050114c8c88ed0 |
| Source note | uspto-grants-2006_06 |