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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1830484Generated: October 30, 2026

Oxalyl chloride → 4-Cyano-3-fluorophenyl 7-propylphenanthrene-2-carboxylate

https://huagongshe.com/reaction/1830484

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
Reactant2-Fluoro-4-hydroxybenzonitrileHCID 2734675—
Reactant2-Propyl-7-(3,4,5-trifluorophenyl)-9,10-dihydrophenanthreneHCID 22044663—
Product4-Cyano-3-fluorophenyl 7-propylphenanthrene-2-carboxylateHCID 21032919—

Reaction Steps

2-iodo-7-propylphenanthrene produced in Example 1 was reacted with oxalyl dichloride, and subsequently reacted with 2-fluoro-4-hydroxybenzonitrile to yield 4-cyano-3-fluorophenyl 7-propylphenanthrene-2-carboxylate

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07067179B1
Source datasetuspto-grants-2006_06
ORD IDord-0af4bddb0b964880b55fb92545a86803
Source noteuspto-grants-2006_06