HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyldimethylsilyl chloride → HCID 22048157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | 4-Bromo-2,6-difluorophenol | HCID 2736292 | — |
| Product | HCID 22048157 | HCID 22048157 | — |
Reaction Steps
The title compound was prepared by reacting 4-bromo-2,6-difluoro-phenol (10.54 g, 50.4 mmol) with TBDMS-Cl (9.88 g, 150.7 mmol) according to method E to yield 14.61 g (90%) of a clear, colorless, oil: 1H NMR (CDCl3) δ 0.17 (6H, s), 0.99 (9H, s), 7.02 (H, d, J=7.13 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067524B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-edf0eb8e2340404ab597799d3e73474c |
| Source note | uspto-grants-2006_06 |