HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 23248656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | (2-Amino-5-bromophenyl)(3-chlorophenyl)methanone | HCID 182478 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23248656 | HCID 23248656 | 120.2% |
Reaction Steps
A solution of intermediate (2) (0.328 mol) and acetic acid, anhydride (0.656 mol) in toluene (1200 ml) was stirred and refluxed for one night. The mixture was evaporated and the product was used without further purification, yielding 139 g (quant.) of N-[4-bromo-2-(3-chlorobenzoyl)phenyl]-acetamide (intermediate 3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067531B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-0dd5cb84192341dc84bd928f2a81474b |
| Source note | uspto-grants-2006_06 |