HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22048468, compound → HCID 22048480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22048468 | HCID 22048468 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22048480 | HCID 22048480 | 214.7% |
Reaction Steps
A mixture of intermediate (7) (0.00141 mol) in HCl 3N (20 ml) and THF (5 ml) was stirred and refluxed overnight. The solvent was evaporated till dryness. The product was used without further purification, yielding 0.73 g (quant.) of 4-(3-chlorophenyl)-6-[hydroxybis(1-methyl-1H-imidazol-5-yl)methyl]-2(1H)-quinolinone hydrochloride (1:2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067531B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-2f5b3a5ec95740d391d40c2fcd10d924 |
| Source note | uspto-grants-2006_06 |