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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1830869Generated: October 31, 2026

Diethyl Ether → HCID 22049722, compound

https://huagongshe.com/reaction/1830869

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
ReactantHCID 22049678HCID 22049678—
ReactantHCID 178418373HCID 178418373—
SolventTetrahydrofuranHCID 8028—
ProductHCID 22049722HCID 22049722—

Reaction Steps

The compound (141) (857 mg, 2.5 mmol) was dissolved in anhydrous tetrahydrofuran (5 ml) and a 2M solution (3 ml, 6.0 mmol) of MeMgI in ether was added under ice-cooling. The reaction mixture was stirred at room temperature for one hr.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07067537B2
Source datasetuspto-grants-2006_06
ORD IDord-6d0020f019c949d7937196c016ceb833
Source noteuspto-grants-2006_06