HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22049743, compound → HCID 22049777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22049743 | HCID 22049743 | — |
| Reactant | 2-Bromo-1-(4-methylpyridin-3-yl)ethan-1-one | HCID 22049783 | — |
| Product | HCID 22049777 | HCID 22049777 | — |
Reaction Steps
By the reaction in the same manner as in Example 25-ii) using 1-oxo-4-isoindolincarbonitrile (310 mg), 1-oxoisoindolin-4-carbothioamide was obtained as pale-green powder. Then, by the reaction in the same manner as in Example 25-iii) using 2-bromo-1-(4-methylpyridin-3-yl)ethanone hydrobromate (520 mg) and 1-oxoisoindolin-4-carbothioamide, the title compound (51 mg) was obtained as colorless powder crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067537B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-a0c2094cd40145548d91fbe5e94e259f |
| Source note | uspto-grants-2006_06 |