HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 22049742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22049750 | HCID 22049750 | — |
| Product | HCID 22049742 | HCID 22049742 | — |
Reaction Steps
By the reaction in the same manner as in Example 60 using 2-fluoro-5-{2-[4-(trifluoromethyl)pyridin-3-yl]-1,3-thiazol-4-yl}benzoic acid (202 mg), thionyl chloride (0.06 ml) and aqueous ethylamine solution (70%, 5 ml), the title compound (139 mg) was obtained as colorless powder crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067537B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-4be9f7f5165b42818d99d9cabf712277 |
| Source note | uspto-grants-2006_06 |