HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylpyridine-3-carbothioamide → HCID 22049790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylpyridine-3-carbothioamide | HCID 22049721 | — |
| Reactant | 2-Bromo-1-(4-methylpyridin-3-yl)ethan-1-one | HCID 22049783 | — |
| Product | HCID 22049790 | HCID 22049790 | 42% |
Reaction Steps
By the reaction in the same manner as in Example 25-iii) using 2-bromo-1-(4-methylpyridin-3-yl)ethanone hydrobromate (392 mg) and 4-methylpyridine-3-thiocarboxamide (152 mg), the title compound (112 mg) was obtained as colorless powder crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067537B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-af99d101f8f24d04bcd2cd8ac64fad21 |
| Source note | uspto-grants-2006_06 |