HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 22049769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22049703 | HCID 22049703 | — |
| Product | HCID 22049769 | HCID 22049769 | — |
Reaction Steps
By the reaction in the same manner as in Example 60 using 3-[2-(4-methyl-pyridin-3-yl)-1,3-thiazol-4-yl]benzoic acid (256 mg), thionyl chloride (0.09 ml) and aqueous methylamine solution (40%, 5 ml), the title compound (191 mg) was obtained as colorless powder crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067537B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-cf0978da721f4382a56f8e5c6493f91c |
| Source note | uspto-grants-2006_06 |