Methacrylic Acid → 1-Butoxyethyl methacrylate

HRID 1831023Notes

Reaction equation

HRID 1831023 reaction equation
[CH2:1]([O:5][CH:6]=[CH2:7])[CH2:2][CH2:3][CH3:4].[C:8]([OH:13])(=[O:12])[C:9]([CH3:11])=[CH2:10]>>[C:8]([O:13][CH:6]([O:5][CH2:1][CH2:2][CH2:3][CH3:4])[CH3:7])(=[O:12])[C:9]([CH3:11])=[CH2:10]

Participants

3

Reactant 2

HCID 4093Methacrylic AcidHCID 8108Butyl vinyl ether

Product 1

HCID 219599501-Butoxyethyl methacrylate

Procedure

The reaction procedure of Example 1 was repeated using equimolar amounts of n-butylvinyl ether and methacrylic acid. The structure of the product, 1-n-butoxyethyl methacrylate (Compound C) was obtained in 88% yield. Compound C is an example of a mono-functional alpha-alkoxyalkyl(meth)acrylate which may optionally be included with multi-functional alpha-alkoxyalkyl(meth)acrylate compounds in compositions of the present invention. The structure of Compound C was confirmed by 1H NMR and infrared analysis.

Workup

  1. customThe reaction procedure of Example 1

Sources & evidence

ORD record
ord-290fa3e56ef54cc2ab37f996c368b87c
Source dataset
uspto-grants-2006_06
Patent number
US07067601B2

Reaction notes

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