Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-trifluoromethylsulfanyl-phenyl Ester

HRID 1831093Notes

Reaction equation

HRID 1831093 reaction equation
[F:1][C:2]([S:5][C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][CH:7]=1)([F:4])[F:3].[CH3:13][N:14]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:15](Cl)=[O:16]>>[F:1][C:2]([S:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][C:15](=[O:16])[N:14]([CH3:13])[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:8][CH:7]=1)([F:4])[F:3]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 38151584-(Trifluoromethylsulfanyl)phenol

Product 1

HCID 10286564Methyl-phenyl-carbamic Acid 4-trifluoromethylsulfanyl-phenyl Ester

Procedure

The title compound was prepared from 4-trifluoromethylsulfanyl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (70%, clear oil). HPLC-MS m/z=328.0 (M+1), Rt: 5.16 min.

Sources & evidence

ORD record
ord-b41cd22b14e24df0a1a50b43e1c51c2b
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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