HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-trifluoromethylsulfanyl-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | 4-(Trifluoromethylsulfanyl)phenol | HCID 3815158 | — |
| Product | Methyl-phenyl-carbamic Acid 4-trifluoromethylsulfanyl-phenyl Ester | HCID 10286564 | — |
Reaction Steps
The title compound was prepared from 4-trifluoromethylsulfanyl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (70%, clear oil). HPLC-MS m/z=328.0 (M+1), Rt: 5.16 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-b41cd22b14e24df0a1a50b43e1c51c2b |
| Source note | uspto-grants-2006_06 |