HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzylphenol → Methyl-phenyl-carbamic Acid 4-benzyl-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzylphenol | HCID 7563 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic Acid 4-benzyl-phenyl Ester | HCID 10125687 | — |
Reaction Steps
The title compound was prepared from 4-benzyl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was recrystallized (ethanol/water) (56%, white crystals). HPLC-MS m/z=318.1 (M+l), Rt: 5.05 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-1c5a8fc24c6f4c39a0354f3ff888fcde |
| Source note | uspto-grants-2006_06 |