Carbamic chloride, N-methyl-N-phenyl- → HCID 10237382, compound

HRID 1831096Notes

Reaction equation

HRID 1831096 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][C:11]([OH:14])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.[CH3:15][N:16]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[C:17](Cl)=[O:18]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[CH:13]=[CH:12][C:11]([O:14][C:17](=[O:18])[N:16]([CH3:15])[C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)=[CH:10][CH:9]=2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 950934-Bromo-4'-hydroxybiphenyl

Product 1

HCID 10237382HCID 10237382, compound

Procedure

The title compound was prepared from 4-bromo-4′-hydroxybiphenyl and N-methyl-N-phenylcarbamoyl chloride. The crude product was recrystallized (ethanol) (72%, white crystals). HPLC-MS m/z=382.0) (M+1), Rt: 5.41 min.

Workup

  1. customThe crude product was recrystallized (ethanol) (72%, white crystals)

Sources & evidence

ORD record
ord-4ac454c17d7f443391919dd133cc5081
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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