HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → HCID 10237382, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | 4-Bromo-4'-hydroxybiphenyl | HCID 95093 | — |
| Product | HCID 10237382 | HCID 10237382 | — |
Reaction Steps
The title compound was prepared from 4-bromo-4′-hydroxybiphenyl and N-methyl-N-phenylcarbamoyl chloride. The crude product was recrystallized (ethanol) (72%, white crystals). HPLC-MS m/z=382.0) (M+1), Rt: 5.41 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-4ac454c17d7f443391919dd133cc5081 |
| Source note | uspto-grants-2006_06 |