Dimethylcarbamoyl Chloride → HCID 23635398, compound

HRID 1831128Notes

Reaction equation

HRID 1831128 reaction equation
[Cl:1][C:2]1[C:3]([O:9][C:10]2[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=2)=[N:4][CH:5]=[C:6]([Cl:8])[CH:7]=1.[CH3:17][N:18]([CH3:22])[C:19](Cl)=[O:20]>>[Cl:1][C:2]1[C:3]([O:9][C:10]2[CH:15]=[CH:14][C:13]([O:16][C:19](=[O:20])[N:18]([CH3:22])[CH3:17])=[CH:12][CH:11]=2)=[N:4][CH:5]=[C:6]([Cl:8])[CH:7]=1

Participants

3

Reactant 2

HCID 6598Dimethylcarbamoyl ChlorideHCID 6208804-(3,5-Dichloro-pyridin-2-yloxy)-phenol

Product 1

HCID 23635398HCID 23635398, compound

Procedure

The title compound was prepared from 4-(3,5-dichloro pyridin-2-yloxy)-phenol and dimethyl-carbamoyl chloride. The crude product was purified by preparative HPLC (38%). HPLC-MS m/z=327.0 (M+1), Rt: 4.7 min.

Workup

  1. customThe crude product was purified by preparative HPLC (38%)

Sources & evidence

ORD record
ord-3caa3b0957eb4300b1dc091c0aa7eab3
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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