HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-acetyl-2-carbamoyl-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | 5-Acetylsalicylamide | HCID 198212 | — |
| Product | Methyl-phenyl-carbamic Acid 4-acetyl-2-carbamoyl-phenyl Ester | HCID 69518900 | — |
Reaction Steps
The title product was prepared from 5-acetylsalicylamide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (87%, white solid). HPLC-MS: m/z=313.1 (M+1); Rt: 2.51 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-5f6f4f3f47b54543a600c89b1625f681 |
| Source note | uspto-grants-2006_06 |