Isoamylamine → HCID 69520146, compound

HRID 1831218Notes

Reaction equation

HRID 1831218 reaction equation
O=C1CCC(=O)N1O[C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([O:16][C:17](=[O:26])[N:18]([CH3:25])[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[CH:12][CH:11]=1.[CH2:28]([NH2:33])[CH2:29][CH:30]([CH3:32])[CH3:31]>>[CH3:31][CH:30]([CH3:32])[CH2:29][CH2:28][NH:33][C:9]([C:10]1[CH:11]=[CH:12][C:13]([O:16][C:17](=[O:26])[N:18]([CH3:25])[C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=2)=[CH:14][CH:15]=1)=[O:27]

Participants

3

Reactant 2

HCID 7894IsoamylamineHCID 865892064-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester

Product 1

HCID 69520146HCID 69520146, compound

Procedure

The title product was prepared from 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester and iso-amylamine. The crude product was used without further purification (95%, oil). HPLC-MS: m/z=341.2 (M+1); Rt: 3.99 min.

Workup

  1. customThe crude product was used without further purification (95%, oil)

Sources & evidence

ORD record
ord-61e893c9a3634f439f8cceb7ba90ee16
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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