huagongshe.com
HRID1831405

反应详情

EQUATION

反应方程式

HRID 1831405 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1ccc(OC(F)(F)F)cc1
HCID2734386

4-(Trifluoromethoxy)phenylboronic acid

C7H6BF3O3

结构：CN(C(=O)Oc1ccc(I)cc1)c1ccccc1
HCID69517304

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(-c2ccc(OC(F)(F)F)cc2)cc1)c1ccccc1
HCID69519252

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from methyl-phenyl-carbamic acid 4-iodo-phenyl ester and 4-trifluoromethoxyphenylboronic acid. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane 1:9) (17%, brown oil).

WORKUP

后处理

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane 1:9) (17%, brown oil)