HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethoxy)phenylboronic acid → Methyl-phenyl-carbamic Acid 4'-trifluoromethoxy-biphenyl-4-yl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethoxy)phenylboronic acid | HCID 2734386 | — |
| Reactant | Methyl-phenyl-carbamic Acid 4-iodo-phenyl Ester | HCID 69517304 | — |
| Product | Methyl-phenyl-carbamic Acid 4'-trifluoromethoxy-biphenyl-4-yl Ester | HCID 69519252 | — |
Reaction Steps
The title compound was prepared from methyl-phenyl-carbamic acid 4-iodo-phenyl ester and 4-trifluoromethoxyphenylboronic acid. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane 1:9) (17%, brown oil).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-1d93516c47b64461b89564ddd43c3992 |
| Source note | uspto-grants-2006_06 |