HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Dithionite → HCID 62705479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Dithionite | HCID 24489 | — |
| Reactant | HCID 22052121 | HCID 22052121 | — |
| Product | HCID 62705479 | HCID 62705479 | 75% |
Reaction Steps
[4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1,2-dimethyl-propyl)-amine (0.26 g, 0.74 mmol) and Na2S2O4 (1.03 g, 5.94 mmol) were treated substantially as described in Part E of Example 9 to yield 0.18 g (75%) of crude 4-(2,4-dichloro-phenyl)-N2-(1,2-dimethyl-propyl)-pyridine-2,3-diamine: MS (AP) m/z 324.3 [(M+H)+, 70].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067658B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-d50332c77f5b4fa9a4a7b351c301e19f |
| Source note | uspto-grants-2006_06 |