HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(1-pyridin-4-ylethyl)formamide → HCID 22052374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(1-pyridin-4-ylethyl)formamide | HCID 2771720 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22052374 | HCID 22052374 | — |
Reaction Steps
N-(1-Pyridin-4-yl-ethyl)-formamide (1.86 g, 12.38 mmol) was dissolved in 50 ml of acetic acid. After addition of Rh (5% on Al2O3, 307 mg) the mixture was hydrogenated with 10 bar hydrogen and 100° C. for 120 hours. The mixture was evaporated and lyophilised. The crude material was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067665B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-e9ad8eb38b184374bd02bcba4d2cf473 |
| Source note | uspto-grants-2006_06 |