HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → 3-Chloropropyl phenyl sulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Product | 3-Chloropropyl phenyl sulfide | HCID 269606 | — |
Reaction Steps
Prepared by Procedure R and Scheme Z using benzenethiol and 1-bromo-3-chloropropane: 1H NMR (400 MHz, CDCl3) δ 7.37–7.34 (m, 2H), 7.32–7.26 (m, 2H), 7.19 (tt, 1H, J=1.4, 7.3 Hz), 3.67 (t, 2H, J=6.6 Hz), 3.08 (t, 2H, J=6.6 Hz), 2.06 (qt, 2H, J=6.6 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067534B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-923c9235f9fd4a5d9a83a573b7b91266 |
| Source note | uspto-grants-2006_06 |