Phenylhydrazine → 2-methyl-N-[3-[1-[(5E)-5-(4-nitrophenyl)-5-(phenylhydrazinylidene)pentyl]piperidin-4-yl]phenyl]propanamide

HRID 1832939Notes

Reaction equation

HRID 1832939 reaction equation
[CH3:1][CH:2]([CH3:33])[C:3]([NH:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]2[CH2:17][CH2:16][N:15]([CH2:18][CH2:19][CH2:20][CH2:21][C:22]([C:24]3[CH:29]=[CH:28][C:27]([N+:30]([O-:32])=[O:31])=[CH:26][CH:25]=3)=O)[CH2:14][CH2:13]2)[CH:7]=1)=[O:4].[C:34]1([NH:40][NH2:41])[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1>>[CH3:1][CH:2]([CH3:33])[C:3]([NH:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]2[CH2:17][CH2:16][N:15]([CH2:18][CH2:19][CH2:20][CH2:21]/[C:22](/[C:24]3[CH:29]=[CH:28][C:27]([N+:30]([O-:32])=[O:31])=[CH:26][CH:25]=3)=[N:41]\[NH:40][C:34]3[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=3)[CH2:14][CH2:13]2)[CH:7]=1)=[O:4]

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 220488632-Methyl-N-(3-{1-[5-(4-nitrophenyl)-5-oxopentyl]-4-piperidinyl}phenyl)propanamide

Product 1

HCID 586513352-methyl-N-[3-[1-[(5E)-5-(4-nitrophenyl)-5-(phenylhydrazinylidene)pentyl]piperidin-4-yl]phenyl]propanamide

Procedure

Prepared by Procedure E and Scheme AX using 2-methyl-N-(3-{1-[5-(4-nitrophenyl)-5-oxopentyl]-4-piperidinyl}phenyl)propanamide and phenylhydrazine: ESMS m/e: 542.4 (M+H)+.

Workup

  1. customPrepared by Procedure E and Scheme AX

Sources & evidence

ORD record
ord-d90d11d9a4b643268961bd20799f98a4
Source dataset
uspto-grants-2006_06
Patent number
US07067534B1

Reaction notes

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