HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 1713031, compound → HCID 22049065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 1713031 | HCID 1713031 | — |
| Reactant | 2-methyl-N-[3-(4-piperidyl)phenyl]propanamide | HCID 16757255 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22049065 | HCID 22049065 | — |
Reaction Steps
Prepared by Procedure F and Scheme R, without HOAc, using 1,9-dimethyl-9H-carbazole-3-carbaldehyde and 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide: 1H NMR (400 MHz, CDCl3) δ 8.05–6.77 (m, 10H) 5.20–5.12 (m, 1H), 4.04 (s, 3H) 3.93 (s, 2H), 3.34–3.24 (m, 2H), 2.79 (s, 3H), 2.56–2.38 (m, 2H), 2.38–2.26 (m, 2H), 2.08–1.88 (m, 2H), 1.82–1.70 (m, 2H), 1.16 (d, 6H, J=6.8 Hz); ESMS m/e: 454.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067534B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-6a01707264164aaba874fc043b248fe6 |
| Source note | uspto-grants-2006_06 |