Potassium Carbonate → HCID 22049088, compound

HRID 1833094Notes

Reaction equation

C([O-])([O-])=O.[K+].[K+].[CH3:7][CH:8]([CH3:24])[C:9]([NH:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH:18]2[CH2:23][CH2:22][NH:21][CH2:20][CH2:19]2)[CH:13]=1)=[O:10].Br[CH2:26][CH2:27][CH2:28][C:29]1[CH:33]=[CH:32][NH:31][CH:30]=1>>[CH3:7][CH:8]([CH3:24])[C:9]([NH:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH:18]2[CH2:23][CH2:22][N:21]([CH2:26][CH2:27][CH2:28][C:29]3[CH:33]=[CH:32][NH:31][CH:30]=3)[CH2:20][CH2:19]2)[CH:13]=1)=[O:10]

Participants

Reactant 3

HCID 11430Potassium Carbonate

HCID 14247124HCID 14247124, compound

HCID 167572552-methyl-N-[3-(4-piperidyl)phenyl]propanamide

Product 1

HCID 22049088HCID 22049088, compound

Procedure

Prepared by Procedure K (KI) and Scheme E (K2CO3) using 2-methyl-N-(3-(4-piperidinyl)phenyl]propanamide and 3-(3-bromopropyl)-1H-pyrrole: ESMS m/e: 354.2 (M+H)+.

Sources & evidence

ORD record: ord-fd65dad38897496fbce800f135570a6f
Source dataset: uspto-grants-2006_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07067534B1

Reaction notes

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