Potassium Carbonate → HCID 22049368, compound

HRID 1833099Notes

Reaction equation

HRID 1833099 reaction equation
C([O-])([O-])=O.[K+].[K+].[CH3:7][CH:8]([CH3:24])[C:9]([NH:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH:18]2[CH2:23][CH2:22][NH:21][CH2:20][CH2:19]2)[CH:13]=1)=[O:10].[Br:25][C:26]1[CH:31]=[CH:30][C:29]([C:32](=[O:37])[CH2:33][CH2:34][CH2:35]Cl)=[CH:28][CH:27]=1>>[Br:25][C:26]1[CH:27]=[CH:28][C:29]([C:32](=[O:37])[CH2:33][CH2:34][CH2:35][N:21]2[CH2:22][CH2:23][CH:18]([C:14]3[CH:13]=[C:12]([NH:11][C:9](=[O:10])[CH:8]([CH3:24])[CH3:7])[CH:17]=[CH:16][CH:15]=3)[CH2:19][CH2:20]2)=[CH:30][CH:31]=1

Participants

4

Reactant 3

HCID 11430Potassium CarbonateHCID 783174'-Bromo-4-chlorobutyrophenoneHCID 167572552-methyl-N-[3-(4-piperidyl)phenyl]propanamide

Product 1

HCID 22049368HCID 22049368, compound

Procedure

Prepared by Procedure K (KI) and Scheme E (K2CO3) using 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide and 1-(4-bromophenyl)-4-chloro-1-butanone: ESMS m/e: 471.3 (M+H)+.

Sources & evidence

ORD record
ord-404328db5fa34ca19298ca0176c2c283
Source dataset
uspto-grants-2006_06
Patent number
US07067534B1

Reaction notes

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