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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1833105Generated: November 2, 2026

Cyclohexanone → HCID 68432283, compound

https://huagongshe.com/reaction/1833105

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexanoneHCID 7967—
Reactant1,3-DioxolaneHCID 12586—
Reactant4'-Hydroxy-4-biphenylcarbonitrileHCID 140610—
CatalystAzobisisobutyronitrileHCID 6547—
ProductHCID 68432283HCID 68432283178.2%

Reaction Steps

A coating solution was prepared for the coating procedure. 8.21 grams of cyanobiphenyl benzoate ethyl acrylate was polymerized with 0.80 grams of LC 756 in 27.1 grams of dioxolane (commercially available from Aldrich Chemical Co., Milwaukee, Wis.) using 0.29 grams of Vazo 52 (commercially available from Dupont, Wilmington, Del.) as a thermal initiator. This reaction was run for 16 hours at 60° C. This solution was then combined with 15 grams of cyclohexanone (commercially available from Aldrich Chemical Co., Milwaukee, Wis.), 15.4 grams of LC 242, 0.64 grams of LC 756, 2.24 grams of 4′-hydroxy-1,1′-biphenyl-4-carbonitrile (commercially available from Aldrich Chemical Co., Milwaukee, Wis.), 27.1 grams of dioxolane (commercially available from Aldrich Chemical Co., Milwaukee, Wis.), 0.11 grams of butylated hydroxyl toluene (BHT is commercially available from Aldrich Chemical Co., Milwaukee, Wis.), 0.28 grams of Irgacure 819 (commercially available from Ciba Geigy, Hawthorne, N.Y.), and 0.84 grams of phenyl ethyl acrylate (commercially available from Polysciences, Warrington, Pa.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07068344B2
Source datasetuspto-grants-2006_06
ORD IDord-0bf0c2da745645f89fc68b311e45feb5
Source noteuspto-grants-2006_06