HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl phosphonoformate → HCID 178485087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl phosphonoformate | HCID 451443 | — |
| Reactant | HCID 178485107 | HCID 178485107 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178485087 | HCID 178485087 | — |
Reaction Steps
A solution of 54 parts of dimethyl methoxycarbonylphosphonate and 33 parts of 1,1,3-trimethylguanidine in 1000 parts of anhydrous tetrahydrofuran was refluxed for one hour. The solvent was removed under reduced pressure to yield 71 parts of dimethyl 1-dimethylamino-1-methylaminomethyleneaminocarbonylphosphonate, nD25 = 1.4989.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04066434 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-5c55fbc9a0ea45d398345fe514c13037 |
| Source note | uspto-grants-1978_01 |