HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Methylisourea → HCID 53677251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Methylisourea | HCID 75544 | — |
| Reactant | Trimethyl phosphonoformate | HCID 451443 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53677251 | HCID 53677251 | — |
Reaction Steps
a mixture of 23 parts of 0-methylisourea and 54 parts of dimethyl methoxycarbonylphosphonate in 1000 parts of anhydrous tetrahydrofuran was refluxed for one hour. The solvent was removed to give dimethyl 1-amino-1-methoxy-methyleneaminocarbonylphosphonate, nD27 = 1.4774.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04066434 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-a39fd5c9341d4daa89d39a40ac6c940a |
| Source note | uspto-grants-1978_01 |