HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 54080401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | Diethyl carbamoylphosphonate | HCID 3692772 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54080401 | HCID 54080401 | — |
Reaction Steps
a solution of 54 parts of diethyl carbamoylphosphonate and 36 parts of dimethyl formamide dimethyl acetal was refluxed in 1000 parts of anhydrous tetrahydrofuran for eight hours. The solvent was removed under reduced pressure to give 70 parts of diethyl 1-dimethylaminomethyleneaminocarbonylphosphonate, nD24 = 1.4970.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04066434 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-604c31e06614499ba55501a3884b2024 |
| Source note | uspto-grants-1978_01 |