HuagongsheHuagongshe Chemistry Print Report · For research reference only
Putrescine → Dodecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Putrescine | HCID 1045 | — |
| Reactant | 1,12-Dodecanediamine | HCID 17727 | — |
| Reactant | 1,8-Octanediamine | HCID 24250 | — |
| Reactant | 1,4-Bis[beta-(3,5-di-t-butyl-4-hydroxy phenyl) propionamido] butane | HCID 14857647 | — |
| Reactant | 3-(3,5-Di-tert-butyl-4-hydroxyphenyl)propionyl chloride | HCID 15606968 | — |
| Reactant | 1,8-Bis[beta-(3,5-di-t-butyl-4-hydroxy phenyl) propionamido] octane | HCID 23337168 | — |
| Product | Dodecane | HCID 8182 | — |
Reaction Steps
Using techniques similar to the one described above 1,4-bis[β-(3,5-di-t-butyl-4-hydroxy phenyl) propionamido] butane (M.P. 203°-205° C); 1,8-bis[β-(3,5-di-t-butyl-4-hydroxy phenyl) propionamido] octane (M.P. 94.5°-96° C); and 1,12-bis[β-3,5-di-t-butyl-4-hydroxy phenyl) propionamido] dodecane (M.P. 89°-92° C) were prepared by reaction of β-(3,5-di-t-butyl-4-hydroxy phenyl) propionyl chloride with respectively 1,4 diamino butane, 1,8-diamino octane and 1,12-diamino dodecane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04066610 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-8ed7d1089d1642dea35085cad8314e99 |
| Source note | uspto-grants-1978_01 |