Hydrogen Peroxide → HCID 178460815, compound

HRID 1833815Notes

Reaction equation

HRID 1833815 reaction equation
[CH2:1](Cl)[CH:2]=[CH2:3].[C:5]([N:7]=[C:8]([S-:10])[S-:9])#[N:6].[K+].[K+].[OH:13]O>>[OH:13][C:5]1[N:7]=[C:8]([S:10][CH2:1][CH:2]=[CH2:3])[S:9][N:6]=1

Participants

4

Reactant 3

HCID 784Hydrogen PeroxideHCID 7850Allyl chlorideHCID 83179Carbamodithioic acid, cyano-, dipotassium salt

Product 1

HCID 178460815HCID 178460815, compound

Procedure

77 g of allyl chloride and 195 g of potassium N-cyanodithioimidocarbonate were condensed and the reaction product was oxidized with 100 ml of 30% hydrogen peroxide to obtain 63 g of 3-hydroxy-5-allylthio-1,2,4-thiadiazole melting at 84° C.

Workup

  1. customcondensed

Sources & evidence

ORD record
ord-3325b01eba064afea9cfb98aa842b405
Source dataset
uspto-grants-1978_01
Patent number
US04067720

Reaction notes

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