HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21388034, compound → HCID 21388032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21388034 | HCID 21388034 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 21388032 | HCID 21388032 | — |
Reaction Steps
1 g of 1-(3-tert.-Butyl-2-phenyl-5-oxazolidinyl-methoxy)-7-chloro-4-methylisoquinoline is heated to 80° in 10 ml of 1N hydrochloric acid for 10 minutes. The reaction mixture is extracted with ether. The ethereal phase is discarded and the aqueous phase worked up to yield the title compound in free base form. M.p. 116°-117°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04067873 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-745197a7ef254b54a06f2dcd24e6ae9a |
| Source note | uspto-grants-1978_01 |